N-甲基二乙醇胺中的阴离子分析

更新时间:2010-10-20  点击次数:2643

N-甲基二乙醇胺阴离子报告

Printing time: Wed Sep 29 12:40:04 2010

Injection time: Wed Sep 29 11:37:55 2010

operator: (temporary), system administrator

分析条件:  :cic-200     流速:1.0ml/min     量程:1

          分离柱:sh-ac      流动相: 碳酸钠    检测方式抑制电导

数据仅供参考,不做判定依据,采用外标法单点校正。

标准品谱图:

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Rank   Time     Name     Quantity   Area        

------------------------------------------------

1      4.475    COOH     2          1135007     

2      5.268    CL       2          2095252     

3      7.928    NO3      2          1022979     

4      13.107   H2PO4    5          1239713     

5      15.043   SO4      3          1908172     

6      16.782   OXALIC   2          10855890    

7      21.006   S2O3     2          13394106    

------------------------------------------------

Total                    18         31651119    

1#样品谱图:

样品稀释2500倍过0.22微米滤膜,进样计算。

File opened: E:\\ÕŽõ÷\\2010\\¶þÒÒ´¼°·\\1# 2500 (20100929 11;37;55).hw

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Rank   Time     Name     Quantity   Area        

------------------------------------------------

1      4.382    COOH     0          0           

2      5.438    CL       36.21      15863       

3      7.724    NO3      0          0           

4      13.488   H2PO4    1.167e+004 1157335     

5      14.568   SO4      0          0           

6      16.401   oxalic   0          0           

7      20.362   s2o3     0          0           

------------------------------------------------

Total                    1.171e+004 1173198     

3#样品谱图:

样品稀释1000倍过0.22微米滤膜,进样计算

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Rank   Time     Name     Quantity   Area        

------------------------------------------------

1      4.604    COOH     86.3       48973       

2      5.442    CL       135.6      142021      

3      7.982    NO3      0          0           

4      13.545   H2PO4    2913       722205      

5      15.523   SO4      207.4      131902      

6      17.407   OXALIC   8.695      47199       

7      21.831   S2O3     22.7       152014      

------------------------------------------------

Total                    3374       1244314     

5#样品谱图:(树脂处理)

样品稀释50倍,过阳离子交换树脂,过0.22微米滤膜,进样计算

------------------------------------------------

Rank   Time     Name     Quantity   Area        

------------------------------------------------

1      4.517    COOH     20.49      232579      

2      5.323    CL       7.445      155995      

3      7.982    NO3      0.9533     9752        

4      13.287   H2PO4    3.711      18401       

5      15.203   SO4      4.314      54877       

6      0.000    OXALIC   0          0           

7      0.000    S2O3     0          0           

------------------------------------------------

Total                    36.91      471604      

5#样品谱图:

样品稀释50倍,过0.22微米滤膜,进样计算

------------------------------------------------

Rank   Time     Name     Quantity   Area        

------------------------------------------------

1      4.563    COOH     23.46      266259      

2      5.365    CL       1.575      33005       

3      7.982    NO3      0          0           

4      13.381   H2PO4    2.479      12293       

5      15.356   SO4      1.63       20731       

6      17.407   OXALIC   0          0           

7      21.831   S2O3     0          0           

------------------------------------------------

Total                    29.14      332288      

2#样品谱图:(稀释10倍)

样品稀释10倍,过0.22微米滤膜,进样计算

------------------------------------------------

Rank   Time     Name     Quantity   Area        

------------------------------------------------

2      4.419    COOH     6.608      3283        

3      5.173    CL       640.7      701710      

6      7.785    NO3      未计算          99010       

7      12.916   H2PO4    未计算          3021572     

8      14.780   SO4      212.8      240990      

9      16.492   oxalic   6.543      35937       

10     20.362   s2o3     0          0           

------------------------------------------------

Total                    866.7      4102502     

4#样品谱图:(稀释10倍)

样品稀释10倍,过0.22微米滤膜,进样计算

------------------------------------------------

Rank   Time     Name     Area%      Area        

------------------------------------------------

1      4.370    COOH     632.2      46206       

2      5.172    CL       1.523e+004 1113462     

3      7.787    NO3      1219       89098       

4      12.897   H2PO4    2.35e+004  1716794     

5      14.791   SO4      7025       513479      

6      16.503   oxalic   1457       106517      

7      20.769   s2o3     939.7      68681       

------------------------------------------------

Total                    50003      3654237     

6#样品谱图:(稀释10倍)

------------------------------------------------

Rank   Time     Name     Area%      Area        

------------------------------------------------

1      4.418    COOH     0.09465    1593        

2      5.178    CL       68.65      1155244     

3      7.803    NO3      5.423      91276       

4      12.861   H2PO4    9.984      168035      

5      14.774   SO4      15.17      255255      

6      16.559   oxalic   0.683      11495       

------------------------------------------------

Total                    100        1682898     

1#样品磷酸二氢根加标

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Rank   Time     Name    Area%      Area        

----------------------------------------------

1     13.568   H2PO4   41.58      9680883     

2     15.421   SO4     1.885      438757      

----------------------------------------------

Total                   100        23279894    

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